HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Cyclohexanone, 2-[2-(3,4-dichlorophenyl)-2-oxoethyl]-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 1-Pyrrolidino-1-cyclohexene | HCID 70768 | — |
| Reactant | 2-Bromo-1-(3,4-dichlorophenyl)ethanone | HCID 244751 | — |
| Product | Cyclohexanone, 2-[2-(3,4-dichlorophenyl)-2-oxoethyl]- | HCID 12270332 | — |
Reaction Steps
(0.19 mole) of 1-pyrrolidino-1-cyclohexene and 51.2 g. (0.19 mole) of 3,4-dichlorophenacyl bromide by the method described in Example 39a gave 32.6 g. (60%) of crystals, m.p. 78°-79° (from ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03931407 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-6c68ce6c129c4a1f9990ef8f4d6453e8 |
| Source note | uspto-grants-1976_01 |