Ethanol → HCID 21569627, compound

HRID 1579901Notes

Reaction equation

HRID 1579901 reaction equation
N1([C:6]2[CH2:10][CH2:9][CH2:8][CH:7]=2)CCCC1.[Br:11][C:12]1[CH:21]=[CH:20][C:15]([C:16](=[O:19])[CH2:17]Br)=[CH:14][CH:13]=1.C([OH:24])C>>[Br:11][C:12]1[CH:21]=[CH:20][C:15]([C:16](=[O:19])[CH2:17][CH:6]2[CH2:7][CH2:8][CH2:9][C:10]2=[O:24])=[CH:14][CH:13]=1

Participants

4

Reactant 3

HCID 702EthanolHCID 74544-Bromophenacyl bromideHCID 81570Pyrrolidine, 1-(1-cyclopenten-1-yl)-

Product 1

HCID 21569627HCID 21569627, compound

Procedure

(0.18 mole) of 1-pyrrolidino-1-cyclopentene and 50 g. (0.18 mole) of p-bromophenacyl bromide by the method described in Example 39a gave 20.8 g. (41%) of crystals, m.p. 59°-61° (from ethanol).

Workup

  1. customgave 20.8 g

Sources & evidence

ORD record
ord-871204794b5b4713bfd7b7b13c038fb8
Source dataset
uspto-grants-1976_01
Patent number
US03931407

Reaction notes

Loading…