Bis(eta-cyclopentadienyl) iron → HCID 178500169, compound

HRID 1579926Notes

Reaction equation

HRID 1579926 reaction equation
[CH-:1]1[CH:5]=[CH:4][CH:3]=[CH:2]1.[CH-:6]1[CH:10]=[CH:9][CH:8]=[CH:7]1.[Fe+2:11].[C:12]([O:19][CH3:20])(=[O:18])[CH2:13][CH2:14][C:15]([CH3:17])=O>CO.C1CCCCC1>[C-:1]1([C:15]([C-:6]2[CH:10]=[CH:9][CH:8]=[CH:7]2)([CH3:17])[CH2:14][CH2:13][C:12]([O:19][CH3:20])=[O:18])[CH:5]=[CH:4][CH:3]=[CH:2]1.[CH-:1]1[CH:5]=[CH:4][CH:3]=[CH:2]1.[Fe+2:11].[CH-:1]1[CH:5]=[CH:4][CH:3]=[CH:2]1.[Fe+2:11]

Participants

4

Reactant 2

HCID 7611Bis(eta-cyclopentadienyl) ironHCID 69354Methyl levulinate

Product 1

HCID 178500169HCID 178500169, compound

Reagents, catalysts & solvents 1

HCID 22386193Methanol cyclohexaneSolvent

Procedure

REACTING FERROCENE AND METHYL LEVULINATE IN THE PRESENCE OF AN ACID SUCH AS POLYPHOSPHORIC ACID AND A METHANOL-CYCLOHEXANE SOLVENT AT A TEMPERATURE OF FROM 76° TO 78°C to produce methyl 4, 4-diferrocenylpentanoate; and

Workup

  1. customA TEMPERATURE OF FROM 76° TO 78°C

Sources & evidence

ORD record
ord-85727d981b594d8fb9534f32b1bbf41c
Source dataset
uspto-grants-1976_01
Patent number
US03932240

Reaction notes

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