HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-phenyl-1-(4-phenylphenyl)methanimine → 2-{4-[2-([1,1'-Biphenyl]-4-yl)ethenyl]phenyl}-5,7-dichloro-1-benzofuran
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-phenyl-1-(4-phenylphenyl)methanimine | HCID 291033 | — |
| Reactant | 5,7-Dichloro-2-(4-methylphenyl)-1-benzofuran | HCID 21496036 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Product | 2-{4-[2-([1,1'-Biphenyl]-4-yl)ethenyl]phenyl}-5,7-dichloro-1-benzofuran | HCID 54411368 | — |
Reaction Steps
Following the procedure given in Example 1b equimolar quantities of the above named 5,7-dichloro-2-(p-tolyl)benzofuran and 4-phenylbenzalaniline were interacted in the presence of potassium tert.-butoxide to give 5,7-dichloro2-{4-[2-(4-biphenylyl)vinyl]phenyl}benzofuran which, following recrystallization from chlorobenzene, melted at 258°-260° C. The wavelength of maximum excitation of this compound was 375 nm., and the wavelength of maximum emission was 431 nm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03932301 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-6d3c01cde329492b82966f7d9c04f748 |
| Source note | uspto-grants-1976_01 |