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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1579935Generated: October 30, 2026

Chloral → Chloral p-chlorophenyl isocyanate dodecyl isocyanate

https://huagongshe.com/reaction/1579935

Reaction equation

Participants

RoleNameHCIDCharge
ReactantChloralHCID 6407—
Reactant4-Chlorophenyl IsocyanateHCID 7693—
ReactantTriphenylphosphineHCID 11776—
ReactantDodecane, 1-isocyanato-HCID 77873—
SolventBenzeneHCID 241—
ProductChloral p-chlorophenyl isocyanate dodecyl isocyanateHCID 86732905—

Reaction Steps

The procedure of Example 82 was repeated, using a mixture of 140 ml. chloral, 7 ml. p-chlorophenyl isocyanate, 2 ml. dodecyl isocyanate and 6.0 ml. of a 1 molar solution of triphenylphosphine in benzene. A tough, clear sheet of chloral/p-chlorophenyl isocyanate/dodecyl isocyanate terpolymer was obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS03932318
Source datasetuspto-grants-1976_01
ORD IDord-81bb9bc8d3c344eead35f1b3b520baf8
Source noteuspto-grants-1976_01