Chloral → HCID 86732905, compound

HRID 1579935Notes

Reaction equation

HRID 1579935 reaction equation
[O:1]=[CH:2][C:3]([Cl:6])([Cl:5])[Cl:4].[Cl:7][C:8]1[CH:13]=[CH:12][C:11]([N:14]=[C:15]=[O:16])=[CH:10][CH:9]=1.[CH2:17]([N:29]=[C:30]=[O:31])[CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH3:28].C1(P(C2C=CC=CC=2)C2C=CC=CC=2)C=CC=CC=1>C1C=CC=CC=1>[O:1]=[CH:2][C:3]([Cl:6])([Cl:5])[Cl:4].[Cl:7][C:8]1[CH:13]=[CH:12][C:11]([N:14]=[C:15]=[O:16])=[CH:10][CH:9]=1.[CH2:17]([N:29]=[C:30]=[O:31])[CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH3:28]

Participants

6

Reactant 4

HCID 6407ChloralHCID 76934-Chlorophenyl IsocyanateHCID 11776TriphenylphosphineHCID 77873Dodecane, 1-isocyanato-

Product 1

HCID 86732905HCID 86732905, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

The procedure of Example 82 was repeated, using a mixture of 140 ml. chloral, 7 ml. p-chlorophenyl isocyanate, 2 ml. dodecyl isocyanate and 6.0 ml. of a 1 molar solution of triphenylphosphine in benzene. A tough, clear sheet of chloral/p-chlorophenyl isocyanate/dodecyl isocyanate terpolymer was obtained.

Workup

  1. additiona mixture of 140 ml

Sources & evidence

ORD record
ord-81bb9bc8d3c344eead35f1b3b520baf8
Source dataset
uspto-grants-1976_01
Patent number
US03932318

Reaction notes

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