HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 54284920, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 54233514 | HCID 54233514 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54284920 | HCID 54284920 | — |
Reaction Steps
A reactor provided with a stirring device, a bromine feed and a calcium chloride tube, is filled with a solution of 6.3 parts of 1-cyano-1-ethoxycarbonyl-4-morpholino-4-phenyl-2-aza-1,3-butadiene in 63 parts by volume of dry methylene chloride. 1.4 parts by weight of ammonia (in the form of a concentrated solution in ethanol) are added at the ambient temperature over a period of three days.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03932404 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-5c64e23592a341fcb0cb7c1ee3374964 |
| Source note | uspto-grants-1976_01 |