HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54233514, compound → HCID 73186001, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54233514 | HCID 54233514 | — |
| Reactant | HCID 86732918 | HCID 86732918 | — |
| Product | HCID 73186001 | HCID 73186001 | — |
Reaction Steps
One operates as in Example 12, but the 6.3 parts of 1-cyano-1-ethoxycarbonyl-4-morpholino-4-phenyl-2-aza-1,3-butadiene are replaced by 6 parts of 1-cyano-1-methoxy-carbonyl-4-morpholino-4-phenyl-2-aza-1,3-butadiene. 3.7 parts of 1-cyano-1-methoxycarbonyl-4-amino-4-phenyl-2-aza-1,3-butadiene are obtained. After recrystallisation from methanol, the product melts at 186°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03932404 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-f12765bbb7a64459bbae0e85854a91d5 |
| Source note | uspto-grants-1976_01 |