HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 73186002, compound → HCID 13638029, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 73186002 | HCID 73186002 | — |
| Reactant | HCID 86732919 | HCID 86732919 | — |
| Product | HCID 13638029 | HCID 13638029 | — |
Reaction Steps
One operates as in Example 15, but the 4 parts of 1-cyano-1-methoxycarbonyl-3-methyl-4-amino-4-phenyl-2-aza-1,3-butadiene are replaced by 3.8 parts of 1-cyano-1-methoxy-carbonyl-4-amino-4-phenyl-2-aza-1,3-butadiene. 3.66 parts of 2-methoxycarbonyl-3-amino-5-phenyl-pyrazine are obtained. After recrystallisation of the product from methanol the melting point is 228°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03932404 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-94de2d1a489e40268c1a0c6724d97b0c |
| Source note | uspto-grants-1976_01 |