HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178522696, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 178525604 | HCID 178525604 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 178522696 | HCID 178522696 | — |
Reaction Steps
4(2-Formyloxyethoxy)-N(1H-tetrazol-5-yl)quinaldamide (2 g) in water (100 ml) and 2N sodium hydroxide (14 ml) was warmed on a steam bath for 15 minutes, and cooled. The solution was acidified to pH 2 with dilute hydrochloric acid. The solid was collected, crystallised from aqueous dimethylformamide and dried, m.p. 261.5°-262° (d).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03932416 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-8dbe606df59642c3b678539d90e6f3a6 |
| Source note | uspto-grants-1976_01 |