HRID1580165

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID96084

N-(3-Chloropropyl)dibutylamine

C11H24ClN

结构：CCn1c2ccc(C(=O)O)cc2c2cc(C(=O)O)ccc21

HCID3797914

9-ethyl-9H-carbazole-3,6-dicarboxylic acid

C16H13NO4

PRODUCTS

生成物

结构：CCCCN(CCCC)CCCOC(=O)c1ccc2c(c1)c1cc(C(=O)OCCCN(CCCC)CCCC)ccc1n2CC.Cl.Cl

HCID68134129

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

催化剂HCID5963

Benzyltrimethylammonium chloride

C10H16ClN

PROCEDURE

实验过程

By the procedure of Example 2, one equivalent of 9-ethylcarbazole-3,6-dicarboxylic acid is allowed to react with two equivalents of 3-dibutylaminopropylchloride in the presence of a catalytic amount of benzyltrimethylammonium chloride to give the product.

WORKUP

后处理

customto give the product

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-afdfcb0c8be04e5c995ea9bef13f1e56
来源数据集: uspto-grants-1976_01
DOI: 10.6084/m9.figshare.5104873.v1
专利: US03932456
来源说明: uspto-grants-1976_01

反应 SMILES

[CH2:1]([N:3]1[C:15]2[CH:14]=[CH:13][C:12]([C:16]([OH:18])=[O:17])=[CH:11][C:10]=2[C:9]2[C:4]1=[CH:5][CH:6]=[C:7]([C:19]([OH:21])=[O:20])[CH:8]=2)[CH3:2].[CH2:22]([N:26]([CH2:31][CH2:32][CH2:33][CH3:34])[CH2:27][CH2:28][CH2:29][Cl:30])[CH2:23][CH2:24][CH3:25]>[Cl-].C([N+](C)(C)C)C1C=CC=CC=1>[ClH:30].[ClH:30].[CH2:1]([N:3]1[C:15]2[CH:14]=[CH:13][C:12]([C:16]([O:18][CH2:29][CH2:28][CH2:27][N:26]([CH2:31][CH2:32][CH2:33][CH3:34])[CH2:22][CH2:23][CH2:24][CH3:25])=[O:17])=[CH:11][C:10]=2[C:9]2[C:4]1=[CH:5][CH:6]=[C:7]([C:19]([O:21][CH2:29][CH2:28][CH2:27][N:26]([CH2:31][CH2:32][CH2:33][CH3:34])[CH2:22][CH2:23][CH2:24][CH3:25])=[O:20])[CH:8]=2)[CH3:2]