3-Chloro-N,N-dimethyl-1-propanamine → HCID 68134589, compound

HRID 1580167Notes

Reaction equation

HRID 1580167 reaction equation
[CH2:1]([N:3]1[C:15]2[CH:14]=[CH:13][C:12]([C:16]([OH:18])=[O:17])=[CH:11][C:10]=2[C:9]2[C:4]1=[CH:5][CH:6]=[C:7]([C:19]([OH:21])=[O:20])[CH:8]=2)[CH3:2].[CH3:22][N:23]([CH3:28])[CH2:24][CH2:25][CH2:26][Cl:27]>[Cl-].C([N+](C)(C)C)C1C=CC=CC=1>[ClH:27].[ClH:27].[CH2:1]([N:3]1[C:15]2[CH:14]=[CH:13][C:12]([C:16]([O:18][CH2:26][CH2:25][CH2:24][N:23]([CH3:28])[CH3:22])=[O:17])=[CH:11][C:10]=2[C:9]2[C:4]1=[CH:5][CH:6]=[C:7]([C:19]([O:21][CH2:6][CH2:5][CH2:4][N:3]([CH3:15])[CH3:1])=[O:20])[CH:8]=2)[CH3:2]

Participants

4

Reactant 2

HCID 669603-Chloro-N,N-dimethyl-1-propanamineHCID 37979149-ethyl-9H-carbazole-3,6-dicarboxylic acid

Product 1

HCID 68134589HCID 68134589, compound

Reagents, catalysts & solvents 1

HCID 5963Benzyltrimethylammonium chlorideCatalyst

Procedure

By the procedure of Example 2, one equivalent of 9-ethylcarbazole-3,6-dicarboxylic acid is allowed to react with two equivalents of 3-dimethylaminopropyl chloride in the presence of a catalytic amount of benzyltrimethylammonium chloride to give the product.

Workup

  1. customto give the product

Sources & evidence

ORD record
ord-4bf4fe5f937e47f1a09a34acf2c04993
Source dataset
uspto-grants-1976_01
Patent number
US03932456

Reaction notes

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