1,3-Dichloro-2-butene → HCID 131709900, 화합물

HRID 1580172노트

반응식

HRID 1580172 반응식
[CH3:1][C:2]1([CH3:30])[CH:29]2[C:24]([CH2:25][NH:26][CH2:27][CH2:28]2)=[C:5]2[C:6]([OH:23])([OH:22])[CH:7]=[C:8]([CH:10]([CH3:21])[CH2:11][CH2:12][CH2:13][C:14]3[CH:19]=[CH:18][C:17]([F:20])=[CH:16][CH:15]=3)[CH:9]=[C:4]2[O:3]1.[Cl:31][CH2:32][CH:33]=[C:34](Cl)C>CN(C)C=O>[CH3:30][C:2]1([CH3:1])[CH:29]2[C:24]([CH2:25][N:26]([CH2:34][CH:33]=[CH:32][Cl:31])[CH2:27][CH2:28]2)=[C:5]2[C:6]([OH:22])([OH:23])[CH:7]=[C:8]([CH:10]([CH3:21])[CH2:11][CH2:12][CH2:13][C:14]3[CH:19]=[CH:18][C:17]([F:20])=[CH:16][CH:15]=3)[CH:9]=[C:4]2[O:3]1

참가 물질

4

반응물 2

HCID 135561,3-Dichloro-2-buteneHCID 131709901HCID 131709901, 화합물

생성물 1

HCID 131709900HCID 131709900, 화합물

시약·촉매·용매 1

HCID 6228Dimethylformamide용매

실험 절차

5,5-Dimethyl-8-(4-p-fluorophenyl-1-methylbutyl)-10-hydroxy-1,2,3,4-tetrahydro-5H[1]benzopyrano[4,3-c]pyridin-10-ol (1 mole) and 1,3-dichloro-2-butene (0.5 mole) were reacted in dimethylformamide as described in Example 7 to give the desired product.

출처 및 근거

ORD 기록
ord-ccf95d84d95c4b609d62699b581b2c58
출처 데이터셋
uspto-grants-1976_01
특허 번호
US03932432

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