HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131709904, compound → HCID 131709903, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131709904 | HCID 131709904 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Ethanol | HCID 702 | — |
| Product | HCID 131709903 | HCID 131709903 | — |
Reaction Steps
5,5-Dimethyl-8-(4-p-fluorophenyl-1-methylbutyl)-2-(2-propynyl)-10-hydroxy-1,2,3,4-tetrahydro-5H[1]benzopyrano [4,3-c]pyridin-10-ol was hydrogenated in ethanol using 5% palladium on carbon as a catalyst. When two equivalents of hydrogen were taken up, the catalyst was filtered and solution concentrated to give the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03932432 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-80ab27823adf47018c2c865f571fc954 |
| Source note | uspto-grants-1976_01 |