Hydroxyamine hydrochloride → HCID 131709909, compound

HRID 1580314Notes

Reaction equation

[F:1][C:2]([F:12])([F:11])[S:3][CH2:4][C:5](=O)[C:6]([CH3:9])([CH3:8])[CH3:7].Cl.[NH2:14][OH:15]>>[F:1][C:2]([F:12])([F:11])[S:3][CH2:4][C:5](=[N:14][OH:15])[C:6]([CH3:9])([CH3:8])[CH3:7]

Participants

Reactant 2

HCID 443297Hydroxyamine hydrochloride

HCID 14144952HCID 14144952, compound

Product 1

HCID 131709909HCID 131709909, compound

Procedure

Using the method of example 2, 1-trifluoromethylthio-3,3-dimethyl-2-butanone was reacted with hydroxylamine hydrochloride to provide the desired oxime, m.p. 94.5° to 96°C.

Sources & evidence

ORD record: ord-ecca3074aea84d0287aba208a383c966
Source dataset: uspto-grants-1976_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03932508

Reaction notes

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