HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → 4-tert-Butylphenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | 2,4-Di-tert-butylphenol | HCID 7311 | — |
| Reactant | 1,3-Benzenedisulfonic acid | HCID 7388 | — |
| Product | 4-tert-Butylphenol | HCID 7393 | 81.2% |
Reaction Steps
Thus, to 2.06 grams of 2,4-ditertiary-butyl phenol was added 0.94 grams of phenol. Then 1% of meta-benzenedisulfonic acid was stirred in with warming and the final mixture was heated to 150°C. for 1.5 hours. Analysis gave 81.2% para-tertiary-butyl phenol. The remaining components were its isomers.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03932537 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-e67f234355064b96835abea4102bdc16 |
| Source note | uspto-grants-1976_01 |