Glycine → HCID 15596998, compound

HRID 1580555Notes

Reaction equation

HRID 1580555 reaction equation
I.[CH3:2][N:3](C)[C:4](=[NH:6])S.[NH2:8][CH2:9][C:10]([OH:12])=[O:11]>[OH-].[NH4+]>[CH3:2][N:3]=[C:4]([NH2:6])[NH:8][CH2:9][C:10]([OH:12])=[O:11]

Participants

4

Reactant 2

HCID 750GlycineHCID 178484401HCID 178484401, compound

Product 1

HCID 15596998HCID 15596998, compound

Reagents, catalysts & solvents 1

HCID 14923Ammonium HydroxideSolvent

Procedure

N,N-dimethylisothiourea hydroiodide (9.5 g., 0.041 mole) was added portionwise to a stirred solution of glycine (4.45 g., 0.0595 mole) in concentrated ammonium hydroxide (40 ml.) at room temperature. The reaction was stirred overnight and the product recovered by filtration as white crystals: 3.0 g., m.p. 230° C. (dec.).

Workup

  1. filtrationthe product recovered by filtration as white crystals

Sources & evidence

ORD record
ord-140ae1ba7ac543579c79048ee309b9b6
Source dataset
uspto-grants-1976_01
Patent number
US03933797

Reaction notes

Loading…