Hydrochloric Acid → HCID 86732979, compound

HRID 1580569Notes

Reaction equation

HRID 1580569 reaction equation
[O:1]1[CH2:6][CH2:5][N:4]([CH2:7][CH:8]([C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][N:20]=2)[C:9]([NH:11][CH2:12][N:13]2[CH2:18][CH2:17][O:16][CH2:15][CH2:14]2)=[S:10])[CH2:3][CH2:2]1.[ClH:25]>C(O)C>[ClH:25].[ClH:25].[ClH:25].[O:1]1[CH2:2][CH2:3][N:4]([CH2:7][CH:8]([C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][N:20]=2)[C:9]([NH:11][CH2:12][N:13]2[CH2:14][CH2:15][O:16][CH2:17][CH2:18]2)=[S:10])[CH2:5][CH2:6]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 15581965HCID 15581965, compound

Product 1

HCID 86732979HCID 86732979, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

One gram of 3-morpholino-N-morpholinomethyl-2-(2-pyridyl)thiopropanamide in ethanol is treated with ethereal hydrogen chloride and the solvents are removed under reduced pressure to give 3-morpholino-N-morpholinomethyl-2-(2-pyridyl)thiopropanamide trihydrochloride.

Workup

  1. customthe solvents are removed under reduced pressure

Sources & evidence

ORD record
ord-4687cfecec8b4d40be9a197759efe35a
Source dataset
uspto-grants-1976_01
Patent number
US03933811

Reaction notes

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