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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1580718Generated: November 4, 2026

Hydroxyamine hydrochloride → HCID 53891326, compound

https://huagongshe.com/reaction/1580718

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydroxyamine hydrochlorideHCID 443297—
ReactantSodium AcetateHCID 517045—
ReactantHCID 21563767HCID 21563767—
SolventEthanolHCID 702—
SolventWaterHCID 962—
ProductHCID 53891326HCID 5389132679%

Reaction Steps

2.5 G of hydroxylamine hydrochloride and 2.5 g of sodium acetate dissolved in 10 ml of water are added to 2 g (0.023 mole) of 1-(2-chlorobenzyl)-3-(2-oxopropyl)indole dissolved in 100 ml of 96% ethyl alcohol. Stirring takes place for 12 hours at 20° and the oxime formed is filtered. The product is recrystallised from di-isopropyl ether.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS03933853
Source datasetuspto-grants-1976_01
ORD IDord-630d8f420b9f4c66a4955f3386d2da5d
Source noteuspto-grants-1976_01