HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl (imidazolidin-2-ylidene)acetate → HCID 68144108, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl (imidazolidin-2-ylidene)acetate | HCID 12377942 | — |
| Reactant | HCID 53707123 | HCID 53707123 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68144108 | HCID 68144108 | 72% |
Reaction Steps
Boiling a solution of 7.4 g of then-2-ylideneacetoacetic acid ethyl ester and 5.2 g of 2-carbethoxymethylideneimidazolidine in 60 ml of ethanol for 6 hours yields 5-methyl-7-(then-2-yl)-1,2,3,7-tetrahydroimidazolo[1,2-a]pyridine-6,8-dicarboxylic acid diethyl ester of melting point 134°C (ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03935220 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-aa8c4b65713d4a3b9150a0f31aabeb57 |
| Source note | uspto-grants-1976_01 |