HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(5-Bromopentyl)benzo[de]isoquinoline-1,3-dione → HCID 131710014, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(5-Bromopentyl)benzo[de]isoquinoline-1,3-dione | HCID 16638791 | — |
| Reactant | 2-(6-bromohexyl)-1H-benz[de]isoquinoline-1,3(2H)-dione | HCID 20364507 | — |
| Reactant | HCID 131710013 | HCID 131710013 | — |
| Product | HCID 131710014 | HCID 131710014 | — |
Reaction Steps
Following the procedure of part (b) of Example 56 but substituting 2-(5-bromopentyl)-1H-benz[de]isoquinoline-1,3(2H)-dione for the 2-(6-bromohexyl)-1H-benz[de]isoquinoline-1,3(2H)-dione, one obtains 2-[5-(3,6-dihydro-4-phenyl-1(2H)-pyridinyl)pentyl]-1H-benz[de]isoquinoline-1,3(2H)-dione, hydrochloride (1:1). The product is purified by recrystallization from n-butanol; m.p. 207°-210°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03935227 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-844d3e18ddae47679135d1c3e2069ff5 |
| Source note | uspto-grants-1976_01 |