HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-Butyl hypochlorite → HCID 131710018, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-Butyl hypochlorite | HCID 521297 | — |
| Reactant | HCID 178468316 | HCID 178468316 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 131710018 | HCID 131710018 | — |
Reaction Steps
The foregoing procedure was repeated, but using 12.1 gms. 1-phenyl-2,3,4-pentanetrione-3-phenylhydrazone, 100 ml. chloroform, and 6 ml. tert-butyl hypochlorite. Upon recrystallization from 100 ml. methanol there was obtained 6.3 gms. of compound having a melting point at 132° to 134°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03935316 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-94f8ef775779447085e47a917c30694f |
| Source note | uspto-grants-1976_01 |