HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Anisoyl chloride → HCID 21561634, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Anisoyl chloride | HCID 7477 | — |
| Reactant | 3-Pyridinemethanol, 5-hydroxy-6-methyl-, hydrochloride | HCID 199187 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 21561634 | HCID 21561634 | — |
Reaction Steps
To a solution of 0.9 g. of 5-hydroxymethyl-2-methyl-3-pyridinol hydrochloride in 5 ml. of anhydrous pyridine was added 0.86 g. of p-anisoyl chloride dropwise under cooling. After standing overnight the resulting mixture was poured into ice water and extracted with chloroform.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03935311 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-15bcc5cc87684b72b11f6ed65c6b3fbf |
| Source note | uspto-grants-1976_01 |