HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → HCID 15619940, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 3-Pyridinemethanol, 5-hydroxy-6-methyl-, hydrochloride | HCID 199187 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 15619940 | HCID 15619940 | — |
Reaction Steps
To a solution of 1.7 g. of 5-hydroxymethyl-2-methyl-3-pyridinol hydrochloride in 10 ml. of dimethylformamide was added a solution of 0.9 g. of 50% sodium hydride in 6 ml. of dimethylformamide. The mixture was stirred at room temperature for 3 hours and to the solution was added 1.25 g. of benzyl chloride and additional stirring was continued overnight at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03935311 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-c8e10cb42a94451b94bf2a89e7eeab74 |
| Source note | uspto-grants-1976_01 |