3-(1-Chloroethyl)pyridine → HCID 178463770, compound

HRID 1581154Notes

Reaction equation

HRID 1581154 reaction equation
CC(Cl)c1cccnc1.NCC1(N2CCCCC2)CCOCC1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(NCC1(N2CCCCC2)CCOCC1)c1cccnc1

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 43608680(4-(Piperidin-1-yl)tetrahydro-2H-pyran-4-yl)methanamine

Product 1

HCID 178463770HCID 178463770, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-0e5399b5617a489e98405c3172c8779d
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

Loading…