HCID 11074835, compound → HCID 178472529, compound

HRID 1581162Notes

Reaction equation

HRID 1581162 reaction equation
CC(Cl)c1cccnc1.CCOC(=O)[C@@H]1[C@H](N)[C@@H]2C=C[C@H]1C2>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CCOC(=O)[C@@H]1[C@H](NC(C)c2cccnc2)[C@@H]2C=C[C@H]1C2

Participants

6

Reactant 2

HCID 11074835HCID 11074835, compoundHCID 149329503-(1-Chloroethyl)pyridine

Product 1

HCID 178472529HCID 178472529, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-7701d29c8a6c426381946f269510fd77
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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