3-(1-Chloroethyl)pyridine → HCID 178464194, compound

HRID 1581173Notes

Reaction equation

HRID 1581173 reaction equation
CC(Cl)c1cccnc1.N#Cc1cccc(OCCCN)c1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(NCCCOc1cccc(C#N)c1)c1cccnc1

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 177890473-(3-Aminopropoxy)benzonitrile

Product 1

HCID 178464194HCID 178464194, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-a97c8e3c525a4fb69115985f9712252f
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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