3-(1-Chloroethyl)pyridine → HCID 178436539, compound

HRID 1581182Notes

Reaction equation

HRID 1581182 reaction equation
CC(Cl)c1cccnc1.FC1(F)CCN(C2CCNCC2)C1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(c1cccnc1)N1CCC(N2CCC(F)(F)C2)CC1

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 534880204-(3,3-Difluoropyrrolidin-1-yl)piperidine

Product 1

HCID 178436539HCID 178436539, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-1d0c26bfce5d4533821d2dd64e343cb4
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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