[1,4']Bipiperidinyl-4-carboxylic acid ethyl ester → HCID 178469187, compound

HRID 1581191Notes

Reaction equation

HRID 1581191 reaction equation
CC(Cl)c1cccnc1.CCOC(=O)C1CCN(C2CCNCC2)CC1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CCOC(=O)C1CCN(C2CCN(C(C)c3cccnc3)CC2)CC1

Participants

6

Reactant 2

HCID 4778238[1,4']Bipiperidinyl-4-carboxylic acid ethyl esterHCID 149329503-(1-Chloroethyl)pyridine

Product 1

HCID 178469187HCID 178469187, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-0ed233b4672d4e9fa314f0eb290f545d
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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