3-(1-Chloroethyl)pyridine → HCID 178436544, compound

HRID 1581197Notes

Reaction equation

HRID 1581197 reaction equation
CC(Cl)c1cccnc1.N#Cc1ccc(OC2CCNCC2)cc1Cl>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(c1cccnc1)N1CCC(Oc2ccc(C#N)c(Cl)c2)CC1

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 179862912-Chloro-4-[(piperidin-4-yl)oxy]benzonitrile

Product 1

HCID 178436544HCID 178436544, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-c75b5c4e4a144e8084798f776a69b7df
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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