3-(1-Chloroethyl)pyridine → HCID 178497442, compound

HRID 1581202Notes

Reaction equation

HRID 1581202 reaction equation
CC(Cl)c1cccnc1.COC(=O)c1cccc2c1CCNC2>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>COC(=O)c1cccc2c1CCN(C(C)c1cccnc1)C2

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 16244395Methyl 1,2,3,4-tetrahydroisoquinoline-5-carboxylate

Product 1

HCID 178497442HCID 178497442, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-fc5d7affee30450fb3fe4dd024b70365
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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