3-(1-Chloroethyl)pyridine → HCID 178436538, compound

HRID 1581213Notes

Reaction equation

HRID 1581213 reaction equation
CC(Cl)c1cccnc1.Clc1ccc(O[C@@H]2CCNC2)nn1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(c1cccnc1)N1CC[C@@H](Oc2ccc(Cl)nn2)C1

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 60137558HCID 60137558, compound

Product 1

HCID 178436538HCID 178436538, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-7552b83201e745538f4904f2fdf438ea
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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