3-(1-Chloroethyl)pyridine → HCID 178436532, compound

HRID 1581224Notes

Reaction equation

HRID 1581224 reaction equation
CC(Cl)c1cccnc1.c1cc2c(cc1CC1CCCNC1)OCO2>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(c1cccnc1)N1CCCC(Cc2ccc3c(c2)OCO3)C1

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 170395273-Benzo[1,3]dioxol-5-ylmethyl-piperidine

Product 1

HCID 178436532HCID 178436532, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-74a0995f2dae45a39c3901a9824dd468
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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