3-(1-Chloroethyl)pyridine → HCID 178424318, compound

HRID 1581228Notes

Reaction equation

HRID 1581228 reaction equation
CC(Cl)c1cccnc1.Cc1ccccc1N1CCNC(C)C1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>Cc1ccccc1N1CCN(C(C)c2cccnc2)C(C)C1

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 20099349HCID 20099349, compound

Product 1

HCID 178424318HCID 178424318, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-72a0b448b8a1474e9eeb9cd6d8ffb165
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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