3-(1-Chloroethyl)pyridine → HCID 178436520, compound

HRID 1581229Notes

Reaction equation

HRID 1581229 reaction equation
CC(Cl)c1cccnc1.Clc1ccc(Br)c2c1CNCC2>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(c1cccnc1)N1CCc2c(Br)ccc(Cl)c2C1

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 661574915-BROMO-8-CHLORO-1,2,3,4-TETRAHYDROISOQUINOLINE

Product 1

HCID 178436520HCID 178436520, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-eb3e0b8436504bc5a25facdb8b970229
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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