3-(1-Chloroethyl)pyridine → HCID 178436550, compound

HRID 1581234Notes

Reaction equation

HRID 1581234 reaction equation
CC(Cl)c1cccnc1.O=C1CNCCN1c1ccc(OC(F)(F)F)cc1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(c1cccnc1)N1CCN(c2ccc(OC(F)(F)F)cc2)C(=O)C1

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 534071391-[4-(Trifluoromethoxy)phenyl]-2-piperazinone

Product 1

HCID 178436550HCID 178436550, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-3624009e3b694b1ab58c016ec44b0aa6
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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