3-(1-Chloroethyl)pyridine → HCID 178428035, compound

HRID 1581236Notes

Reaction equation

HRID 1581236 reaction equation
CC(Cl)c1cccnc1.Cc1cc(N2CCNCC2)nc(C(F)(F)F)n1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>Cc1cc(N2CCN(C(C)c3cccnc3)CC2)nc(C(F)(F)F)n1

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 336979354-Methyl-6-piperazin-1-yl-2-(trifluoromethyl)pyrimidine

Product 1

HCID 178428035HCID 178428035, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-6cfeaa2d533c41b181d97512d31a8146
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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