3-(1-Chloroethyl)pyridine → HCID 178436561, compound

HRID 1581239Notes

Reaction equation

HRID 1581239 reaction equation
CC(C)(C)OC(=O)N1CCc2[nH]nc(O)c2C1.CC(Cl)c1cccnc1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(c1cccnc1)n1nc(O)c2c1CCN(C(=O)OC(C)(C)C)C2

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 178451664HCID 178451664, compound

Product 1

HCID 178436561HCID 178436561, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-e99309e3abf1455a9546fdae4e98ebfd
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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