2-Methyl-5-hydroxypyridine → HCID 178426849, compound

HRID 1581247Notes

Reaction equation

HRID 1581247 reaction equation
CC(Cl)c1cccnc1.Cc1ccc(O)cn1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>Cc1ccc(OC(C)c2cccnc2)cn1

Participants

6

Reactant 2

HCID 142752-Methyl-5-hydroxypyridineHCID 149329503-(1-Chloroethyl)pyridine

Product 1

HCID 178426849HCID 178426849, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-aaa9e1f532b54af99963d867ae511d41
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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