2-Nitro-4-(trifluoromethyl)phenol → HCID 178466561, compound

HRID 1581253Notes

Reaction equation

HRID 1581253 reaction equation
CC(Cl)c1cccnc1.O=[N+]([O-])c1cc(C(F)(F)F)ccc1O>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(Oc1ccc(C(F)(F)F)cc1[N+](=O)[O-])c1cccnc1

Participants

6

Reactant 2

HCID 98162-Nitro-4-(trifluoromethyl)phenolHCID 149329503-(1-Chloroethyl)pyridine

Product 1

HCID 178466561HCID 178466561, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-c23c5b5088fe41d68b4252dbb036ca81
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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