3-(1-Chloroethyl)pyridine → HCID 178500719, compound

HRID 1581255Notes

Reaction equation

HRID 1581255 reaction equation
CC(Cl)c1cccnc1.COC(=O)C[C@@H]1COc2cc(O)ccc21>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>COC(=O)C[C@@H]1COc2cc(OC(C)c3cccnc3)ccc21

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 53393313(S)-Methyl 2-(6-hydroxy-2,3-dihydrobenzofuran-3-yl)acetate

Product 1

HCID 178500719HCID 178500719, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-77bfc66f457f465b9a712dea5212c240
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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