2-Cyano-6-hydroxybenzothiazole → HCID 178466036, compound

HRID 1581261Notes

Reaction equation

HRID 1581261 reaction equation
CC(Cl)c1cccnc1.N#Cc1nc2ccc(O)cc2s1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(Oc1ccc2nc(C#N)sc2c1)c1cccnc1

Participants

6

Reactant 2

HCID 98819122-Cyano-6-hydroxybenzothiazoleHCID 149329503-(1-Chloroethyl)pyridine

Product 1

HCID 178466036HCID 178466036, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-fb71bffc3c714423953da6c25f48cb76
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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