7-Hydroxy-2,2,5-trimethyl-2,3-dihydro-4H-1-benzopyran-4-one → HCID 178428995, compound

HRID 1581282Notes

Reaction equation

HRID 1581282 reaction equation
CC(Cl)c1cccnc1.Cc1cc(O)cc2c1C(=O)CC(C)(C)O2>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>Cc1cc(OC(C)c2cccnc2)cc2c1C(=O)CC(C)(C)O2

Participants

6

Reactant 2

HCID 27279647-Hydroxy-2,2,5-trimethyl-2,3-dihydro-4H-1-benzopyran-4-oneHCID 149329503-(1-Chloroethyl)pyridine

Product 1

HCID 178428995HCID 178428995, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-ba7f409f30f749e989fd5bb467304581
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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