2,3-Dihydro-2,2-dimethyl-7-benzofuranol → HCID 178466061, compound

HRID 1581290Notes

Reaction equation

HRID 1581290 reaction equation
CC(Cl)c1cccnc1.CC1(C)Cc2cccc(O)c2O1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(Oc1cccc2c1OC(C)(C)C2)c1cccnc1

Participants

6

Reactant 2

HCID 152782,3-Dihydro-2,2-dimethyl-7-benzofuranolHCID 149329503-(1-Chloroethyl)pyridine

Product 1

HCID 178466061HCID 178466061, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-3576e6423f234917a75a3e37124f6ff9
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

Loading…