(+-)-3-Quinuclidinol → HCID 178467056, compound

HRID 1581309Notes

Reaction equation

HRID 1581309 reaction equation
CC(Cl)c1cccnc1.OC1CN2CCC1CC2>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(OC1CN2CCC1CC2)c1cccnc1

Participants

6

Reactant 2

HCID 15381(+-)-3-QuinuclidinolHCID 149329503-(1-Chloroethyl)pyridine

Product 1

HCID 178467056HCID 178467056, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-7963f9ae644d40a195de142b085b0beb
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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