3-(1-Chloroethyl)pyridine → HCID 178468178, compound

HRID 1581315Notes

Reaction equation

HRID 1581315 reaction equation
CC(Cl)c1cccnc1.CN(C)[C@H]1CC[C@H](O)CC1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(O[C@H]1CC[C@H](N(C)C)CC1)c1cccnc1

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 178484116HCID 178484116, compound

Product 1

HCID 178468178HCID 178468178, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-98996a2ed216482283a0ae46b332c05a
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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