3-(1-Chloroethyl)pyridine → HCID 178428512, compound

HRID 1581321Notes

Reaction equation

HRID 1581321 reaction equation
CC(Cl)c1cccnc1.CC1CCN(CCCO)CC1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC1CCN(CCCOC(C)c2cccnc2)CC1

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 151665833-(4-Methylpiperidin-1-yl)propan-1-ol

Product 1

HCID 178428512HCID 178428512, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-c8b6920ece16430fb3ffdf9c26908348
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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