3-[(2-Hydroxyethyl)sulfanyl]-6-nitro-2,3-dihydro-1H-1-benzothiophene-1,1-dione → HCID 178468140, compound

HRID 1581322Notes

Reaction equation

HRID 1581322 reaction equation
CC(Cl)c1cccnc1.O=[N+]([O-])c1ccc2c(c1)S(=O)(=O)CC2SCCO>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(OCCSC1CS(=O)(=O)c2cc([N+](=O)[O-])ccc21)c1cccnc1

Participants

6

Reactant 2

HCID 27792373-[(2-Hydroxyethyl)sulfanyl]-6-nitro-2,3-dihydro-1H-1-benzothiophene-1,1-dioneHCID 149329503-(1-Chloroethyl)pyridine

Product 1

HCID 178468140HCID 178468140, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-97c612900b4444249c055bacc5da4305
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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