ethyl 4-(2-hydroxyethyl)piperazine-1-carboxylate → HCID 178473362, compound

HRID 1581326Notes

Reaction equation

HRID 1581326 reaction equation
CC(Cl)c1cccnc1.CCOC(=O)N1CCN(CCO)CC1>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CCOC(=O)N1CCN(CCOC(C)c2cccnc2)CC1

Participants

6

Reactant 2

HCID 228934ethyl 4-(2-hydroxyethyl)piperazine-1-carboxylateHCID 149329503-(1-Chloroethyl)pyridine

Product 1

HCID 178473362HCID 178473362, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-6d92a44594104f5d99f3655448ee9deb
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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