3-(1-Chloroethyl)pyridine → HCID 178468643, compound

HRID 1581347Notes

Reaction equation

HRID 1581347 reaction equation
CC(Cl)c1cccnc1.CN(C)Cc1c[nH]c2cc(C(=O)O)ccc12>CN(C)C=O.O=C([O-])[O-].[Cs+].[Cs+].[I-].[K+]>CC(OC(=O)c1ccc2c(CN(C)C)c[nH]c2c1)c1cccnc1

Participants

6

Reactant 2

HCID 149329503-(1-Chloroethyl)pyridineHCID 17967057HCID 17967057, compound

Product 1

HCID 178468643HCID 178468643, compound

Reagents, catalysts & solvents 3

HCID 4875Potassium IodideReagentHCID 10796Cesium carbonateReagentHCID 6228DimethylformamideSolvent3×

Conditions

Temperature
70 °C

Workup

  1. aliquotNo procedure recorded
  2. additionDilution of the aliquot (2 uL) with DMSO (200 uL).

Sources & evidence

ORD record
ord-14e637aada7c45bdb3866590966a0d4f
Source dataset
Fig 7 data from Golden paper
Original link
View source

Reaction notes

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